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TiCl 3 -Enhanced NaAlH 4 : Impact of Excess Al and Development of the Al 1- y Ti y Phase during Cycling

✍ Scribed by Brinks, Hendrik W.; Sulic, Martin; Jensen, Craig M.; Hauback, Bjørn C.

Book ID
126865603
Publisher
American Chemical Society
Year
2006
Tongue
English
Weight
132 KB
Volume
110
Category
Article
ISSN
0022-3654

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Structural properties of the nanoscopic
Structural properties of the nanoscopic Al85Ti15 solid solution observed in the hydrogen-cycled NaAlH4 + 0.1TiCl3 system
✍ M.P. Pitt; P.E. Vullum; M.H. Sørby; M.P. Sulic; C.M. Jensen; J.C. Walmsley; R. H 📂 Article 📅 2008 🏛 Elsevier Science 🌐 English ⚖ 676 KB

The twice-hydrogen-cycled NaAlH 4 + xTiCl 3 (x < 0.15) system has been studied by high-resolution X-ray synchrotron diffraction and transmission electron microscopy. Intense low d-spacing shoulders are formed on Al reflections, indicating the formation of a face-centred cubic Al 85 Ti 15 solid solut