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Through-space R3-HETCOR experiments between spin-1/2 and half-integer quadrupolar nuclei in solid-state NMR

โœ Scribed by J. Trebosc; B. Hu; J.P. Amoureux; Z. Gan


Book ID
108184829
Publisher
Elsevier Science
Year
2007
Tongue
English
Weight
390 KB
Volume
186
Category
Article
ISSN
1090-7807

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Measurement of through-space connectivit
โœ J. P. Amoureux; J. Trรฉbosc; G. Tricot ๐Ÿ“‚ Article ๐Ÿ“… 2007 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 312 KB

We present the transferred echo double-resonance multiple-quantum MAS (TEDOR-MQMAS) method that allows to analyze under high resolution the through-bond connectivities between spin-1/2 and quadrupolar nuclei. This method avoids some of the limitations related to the spin-lock of half-integer quadrup