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Three metal–organic coordination compounds based on 4,6-dipyridyl-2-aminopyrimidine: Important role of hydrogen bonding in supramolecular assemblies

✍ Scribed by Ying-Nan Chi; Feng-Yun Cui; Yan-Qing Xu; Chang-Wen Hu


Publisher
Elsevier Science
Year
2008
Tongue
English
Weight
942 KB
Volume
875
Category
Article
ISSN
0022-2860

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✦ Synopsis


The reactions of divalent metal salts and 4,6-dipyridyl-2-aminopyrimidine ligands gave rise to three metal-organic coordination compounds:

aminopyrimidine] and their crystal structures were determined via single-crystal X-ray diffraction. In the three structures, L1 and L2 both exhibit terminal coordination mode. As the ligands contain both hydrogen bonding donors and acceptors, hydrogen bonding interactions play a crucial role in construction of supramolecular structures. In compound 1, the mono-nuclear complexes were connected to dimer structure by hydrogen bondings; in compound 2, dimer units were constructed through intermolecular hydrogen bondings and the crystallographic water molecules link the dimers into a 1-D supramolecular chain; and in compound 3, a complicated 3-D supramolecular architecture was formed via a series of hydrogen bondings. Moreover, the compounds 1-3 display room-temperature luminescent properties.