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Thermogravimetric analysis for boiling points and vapour pressure

✍ Scribed by J. W. Goodrum; E. M. Siesel

Book ID
105424640
Publisher
Springer Netherlands
Year
1996
Tongue
English
Weight
372 KB
Volume
46
Category
Article
ISSN
0022-5215

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✦ Synopsis

A TGA instrument has been adapted for rapid measurement of boiling points and vapour pressure at temperatures from ambient up to 400~ and pressures from ambient down to 20 mm Hg. Samples were contained in sealed holders having a laser-drilled aperture. Several organic liquids in the 100 to 300 g MW range showed good agreement with reference vapour pressure data. Sample mass, heating rate, and use of inert diluents were important variables affecting accuracy of vapour pressure measurements.

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