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Thermal methods for the synthesis of thiophene, selenophene, and their derivatives. (Review)

✍ Scribed by E. N. Deryagina; M. G. Voronkov

Book ID
105516622
Publisher
Springer US
Year
2000
Tongue
English
Weight
603 KB
Volume
36
Category
Article
ISSN
0009-3122

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## Abstract Naphthalene‐1‐sulfonic acid dimethylamides were treated with __n__‐BuLi and elemental sulfur or selenium to afford dinaphtho[1,2‐__b__:2β€²,1′‐__d__]thiophenes and selenophenes, respectively. This is the first example of making two Cο£ΏS/Se bonds and a Cο£ΏC bond in a single step at room temp