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Thermal dehydration and structural models of two new vanadyl sulfate hydrates

✍ Scribed by R. Schneider; J.R. Günter; H.R. Oswald

Book ID
107819195
Publisher
Elsevier Science
Year
1982
Tongue
English
Weight
473 KB
Volume
45
Category
Article
ISSN
0022-4596

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Two new organic monophosphates, C3H12N 2؉ 2 • HPO 2؊ 4 • H2O (DAPHP) and C6H18N 2؉ 3 • 2HPO ؊ 4 • 4H2O (TMEDH2P), are obtained by action of H3PO4 with respectively 1,2-diaminopropane and N,N,N,N-tetramethylethylenediamine. DAPHP is monoclinic, P21/n, with a ‫؍‬ 10.653(3) A s , b ‫؍‬ 6.025(1) A s , c