Thermal Behaviour of Kaolinite Intercalated with Formamide, Dimethyl Sulphoxide and Hydrazine
✍ Scribed by J. Kristóf; R. L. Frost; J. T. Kloprogge; E. Horváth; M. Gábor
- Book ID
- 110287333
- Publisher
- Springer Netherlands
- Year
- 1999
- Tongue
- English
- Weight
- 222 KB
- Volume
- 56
- Category
- Article
- ISSN
- 0022-5215
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Raman spectra of kaolinite and of the formamide-intercalated kaolinite were obtained at both 298 and 77 K using a Raman microprobe equipped with a thermal stage. Upon cooling to 77 K, the band attributed to the inner hydroxyl shifts by 5 cm-1 to lower wavenumbers and the bands assigned to the inner
Abstractz lhe acyclic and cyclic &&oxydithioarcrals 3u-m and lo-b obtained by sodium borohydride redudion (or Grignam' addition) of the corresponding &oxodithioacetals 2u-m arc shown to undergo facik one pot thermal &h#ration and dethioacetalization in the presenoz of dbnuhyl sulphoxide to &mi the c