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Thermal and hydrothermal stability of molecular sieve VPI-5 by in situ x-ray powder diffraction

✍ Scribed by Annen, Michael J.; Young, David; Davis, Mark E.; Cavin, O. Burl; Hubbard, Camden R.

Book ID
125968268
Publisher
American Chemical Society
Year
1991
Tongue
English
Weight
483 KB
Volume
95
Category
Article
ISSN
0022-3654

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The synthesis of DPA-VPI-5 and TBA-VPI-5 and their phase transformation to AIPO4-8 have been studied by X-ray diffraction in situ. The synchrotron radiation-energy dispersive diffraction is shown to be able to monitor these two fast reactions in real time. The results indicate that nucleation may oc