The X-ray crystal structure of a novel Schiff base macrocycle containing a tricyclic (7 + 12 + 7) inner ring system
β Scribed by de O. Cabral, Joao; Cabral, Maria Fernanda; Drew, Michael G. B.; Esho, Ferida S.; Haas, Otto; Nelson, S. Martin
- Book ID
- 117995770
- Publisher
- The Royal Society of Chemistry
- Year
- 1982
- Tongue
- English
- Weight
- 235 KB
- Volume
- 18
- Category
- Article
- ISSN
- 0022-4936
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Attempted intramolecular pinacolization of cage diketone 4 unexpectedly gave ketol 5 instead. % Compound 5 was shown to possess the rare tetracyclo[4.2.?.1.2,503~7]decane ring system by means of an X-ray crystal structure of hydroxy-mesylate J&j derived from 2 by sodium borohydride reduction follow
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