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The x-ray crystal and molecular structure of chloro-α,β,γ,δ-tetraphenylporphinatopyridinegallium(III)

✍ Scribed by K. M. Radish; J.-L. Cornillon; J. D. Korp; R. Guilard


Book ID
112129347
Publisher
Journal of Heterocyclic Chemistry
Year
1989
Tongue
English
Weight
303 KB
Volume
26
Category
Article
ISSN
0022-152X

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CH,(18) + 14-CH3; 2.07, s CH,( 4) (CDCI,);not yet crystalli~ed]~). Finally, 8 was converted by catalytic hydrogenation [5%-Pd/C in ethanol/triethylamine; + 11 and cyclisation [HCl in acetic acid] into 3-oxo-17~-acetoxy-14a-methyl-A4-8a,9B,lOa,13a-estrene (12) [m.p. 86-88'; -[ U ] D = + 1' (CHC1,).