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The vilsmeier-haack reaction. IV. Reaction of phosphorus oxychloridedimethylformamide with semicarbazones

✍ Scribed by M. A. Kira; M. N. Aboul-Enein; M. I. Korkor


Book ID
112122062
Publisher
Journal of Heterocyclic Chemistry
Year
1970
Tongue
English
Weight
160 KB
Volume
7
Category
Article
ISSN
0022-152X

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The vilsmeier-haack reaction-VI reaction
✍ M.A. Kira; Z.M. Nofal; K.Z. Gadalla πŸ“‚ Article πŸ“… 1970 πŸ› Elsevier Science 🌐 French βš– 158 KB

Acetophenolle anilreactedwith cna mole ofPCCl53DM, inIMP2, and afforded after treawt rith perohlorio acid, the salt Ia, m.p. 160Β°, which upcm azlrrlina i&ydrol,ymir,gmva the x-for@m"ldnrr IIa3,B.p.1300. Tbs mtxuoture of IIaru inferred frcm ita IR (1660 or?) and lDllIL rpectra (CDC13)r ai@alm at 4.5