The use of variable temperature and magic-angle sample spinning in studies of fulvic acids
✍ Scribed by William L Earl; Robert L Wershaw; Kevin A Thorn
- Publisher
- Elsevier Science
- Year
- 1987
- Weight
- 947 KB
- Volume
- 74
- Category
- Article
- ISSN
- 0022-2364
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## Abstract Application of rapid sample rotation and radiofrequency irradiation in magic angle spinning (MAS) NMR of lipid bilayers can significantly increase the sample temperature. In this work, we studied the extent of heating during the acquisition of ^1^H‐decoupled ^13^C MAS spectra of hydrate
A study of the residual dipolar 15 N, 14 N coupling observed in 15 N cross-polarization magic angle spinning NMR spectra at variable temperature and variable field in 1-amino-and 1-nitropyrazole is reported. Residual dipolar 15 N, 14 N coupling is present in high-resolution 15 N spectra as an asymme