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The use of tris(2-aminoethyl)amine in macrocyclization processes

✍ Scribed by Piotr Lipkowski; Daniel T. Gryko; Janusz Jurczak; Janusz Lipkowski

Publisher: Elsevier Science
Year: 1998
Tongue: French
Weight: 190 KB
Volume: 39
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(98)00624-8

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✦ Synopsis

Reactions of tripodal amine I with tripodal esters 2 and 4, carried out in methanol under ambient conditions, afforded -as single products -tricyclic cryptands 3 and 5, respectively. Under the same conditions, the amine 1 reacted with dipodal esters 6 and 7 to give bis-macrocycles 9 and 10, respectively.

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