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The use of sodium tetraethylborate in the derivatization of octyltin compounds

✍ Scribed by Peter J. Craig; Darren Mennie


Publisher
John Wiley and Sons
Year
1994
Tongue
English
Weight
187 KB
Volume
8
Category
Article
ISSN
0268-2605

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✦ Synopsis


Octyltin trichloride (OctSnCI,) and dioctyltin dichloride (Oct,SnCI,) have been reacted with sodium tetraethylborate (NaBEt,) to yield the volatile tetraalkyltin derivatives OctSnEt, and Oct2SnEt2. Single and mixed solutions of the octyltin chlorides have been derivatized, separated and quantified using interfaced GCAA and GCMS methodology.


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