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The use of high-pressure liquid chromatography in the simultaneous assay of 11β-hydroxylase and 18-hydroxylase in zona fascloulata-retioularis tissue of the rat adrenal cortex

✍ Scribed by Samuel Gallant; Sally M. Bruckheimer; Alexander C. Brownie


Publisher
Elsevier Science
Year
1978
Tongue
English
Weight
425 KB
Volume
89
Category
Article
ISSN
0003-2697

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✦ Synopsis


An isocratic, reverse-phase system for determining adrenal cortical steroids by high-pressure liquid chromatography is described. The method enables the rapid, accurate, and precise separation and quantitation of the major steroids produced during in vitro incubations of rat adrenal cortex mitochondria with 1 I-deoxycorticosterone.

The application of this method to the determination of lip-and IS-hydroxylase activity in the presence of metopirone is illustrated, and its utility for studying other enzymatic reactions in the adrenal gland is discussed.