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The use of a lyotropic liquid-crystalline medium and residual dipolar coupling constants for determination of the spatial structure of thiacalix[4]arenes in solutions

✍ Scribed by V. V. Klochkov; B. I. Khairutdinov; A. V. Klochkov; M. S. Tagirov; C. M. Thiele; S. Berger; I. S. Vershinina; I. I. Stoikov; I. S. Antipin; A. I. Konovalov

Book ID
111607773
Publisher
Springer
Year
2004
Tongue
English
Weight
279 KB
Volume
53
Category
Article
ISSN
1573-9171

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The rα-structure of partially oriented 1,2,3,5-tetrachlorobenzene determined from its 1H NMR spectra with natural-abundance 13C-satellites. A Demonstration of the Combined Use of Spectra Obtained from Molecules Dissolved in Several Different Liquid Crystals as Solvents for Spin Systems not having enough Dipolar Coupling Constants to Determine the Molecular Structure
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## Abstract It is demonstrated that in a case where neither the proton nor the natural‐abundance ^13^C‐satellite spectra of a partially oriented molecule carry enough structural information, one can determine the entire molecular geometry by the combined use of several liquid crystals as solvents.