The Triolide of (R)-3-Hydroxybutyric acid—Direct Preparation from Polyhydroxybutyrate and Formation of a Crown Estercarbonyl Complex with Na Ions
✍ Scribed by Prof. Dr. Dieter Seebach; Dipl.-Chem. Hans-Martin Müller; Dipl.-Chem. H. Michael Bürger; Mag. rer. nat. Dietmar A. Plattner
- Book ID
- 101554515
- Publisher
- John Wiley and Sons
- Year
- 1992
- Tongue
- English
- Weight
- 274 KB
- Volume
- 31
- Category
- Article
- ISSN
- 0044-8249
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✦ Synopsis
C(102) to C(l05)l were refined anisotropically. Bonds o f the disordered THF were constrained during refinements. No attempts were made to locate the H atoms. The final refinement of 1 converged at R = 0.053, UR = 0.081, and COF = 2.78 for observed reflections. The maximum and minimum residual electron densities are 0.94 and -0.85 ejA', respectively.
Further details of the crystal structure investigation may be obtained from the Fachinformationszentrum Karlsruhe. Gesellschaft fur wissenschaftlich-technische Information mbH, D-W-7514 Eggenstein-Leopoldshafen 2 (FRG), on quoting the depository number CSD-56000. the names of the authors, and the journal citation.