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The synthesis of several tert-butyloxycarbonyl derivatives of insulin

โœ Scribed by Daniel Levy


Book ID
118847047
Publisher
Elsevier Science
Year
1973
Weight
351 KB
Volume
328
Category
Article
ISSN
0005-2795

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Synthesis of N-tert-Butyloxycarbonyl- an
โœ Dr.-Ing. B. Rzeszotarska; Mgr. S. Wiejak ๐Ÿ“‚ Article ๐Ÿ“… 1968 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 233 KB ๐Ÿ‘ 1 views

residue is treated with ice. The aqueous suspension is extracted with benzene (about 300 ml), and the organic phase is at once chromatographed on acid A1203. Benzene (1000 ml) is used for elution. After evaporation of the solvent the residue is taken up in ether, and the solution is decanted at once