The synthesis of chlorodeoxyhexofuranoid
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Haralambos Parolis
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Article
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1983
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Elsevier Science
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English
⚖ 749 KB
The reaction of 1,2-O-isopropylidene-cc-D-glucofuranose with sulfuryl chloride at 0' and at 50' afforded 6-chloro-6-deoxy-1,2-O-isopropylidene-a-D-glucofuranose 3,5-bis(chlorosulfate) (3) and 5,6-dichloro-5,6-dideoxy-1,2-O-isopropylidene+Lidofuranose 3-chlorosulfate (7, not characterised), respecti