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THE SYNTHESIS OF DIBENZ[ a , c ][1,3]CYCLOHEPTADIENE - 5,7-DIONE

โœ Scribed by Lucien, Harold W.; Taurins, Alfred


Book ID
118182710
Publisher
NRC Research Press
Year
1952
Tongue
French
Weight
650 KB
Volume
30
Category
Article
ISSN
0008-4042

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A novel synthesis of 3-(substituted)pyri
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An improved synthesis of 3-(substituted)pyrimido[4,5-c]pyridazine-5,7(1H,6H)-diones, a known subclass of 4-deazatoxoflavins, is reported. The approach involves treatment of 3-methyl-6-(1-methylhydrazinyl)uracil with representative phenyl and alkyl glyoxal monohydrates, which in turn are obtained by