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The Synthesis of anti-Fixed 3-Methyl-3-deaza-2′-deoxyadenosine and Other 3H-Imidazo[4,5-c]pyridine Analogues.

✍ Scribed by Rostem J. Irani; John SantaLucia Jr.

Book ID
101940359
Publisher
John Wiley and Sons
Year
2003
Weight
217 KB
Volume
34
Category
Article
ISSN
0931-7597

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✦ Synopsis

Abstract

For Abstract see ChemInform Abstract in Full Text.

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## Abstract The synthesis of 4‐(methylthio)‐1__H__‐imidazo[4,5‐__c__]pyridine 2′‐deoxy‐β‐D‐ribonucleosides 2 and 9 and the conversion of the __N__^1^‐isomer 2 into the 2′,3′‐didehydro‐2′,3′‐dideoxyribonucleoside 3a or (__via__ 7) 3‐deaza‐2′‐deoxyadenosine (1) is described. Phosphonate building bloc

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## Abstract The convergent syntheses of 3‐deazapurine 2′‐deoxy‐β‐D‐ribonucleosides and 2′,3′‐dideoxy‐D‐ribonucleosides, including 3‐deaza‐2′‐deoxyadenosine (1a) and 3‐deaza‐2′,3′‐dideoxyadenosine (1b) is described. The 4‐chloro‐l__H__‐imidazo[4,5‐c]pyridinyl anion derived from 5 was reacted with ei