THE SYNTHESIS ## Errufn. I%\' JOIIN W. CODU.
The synthesis of a glaze, glass, or other complex silicate
β Scribed by Cobb, John W.
- Publisher
- Wiley (John Wiley & Sons)
- Year
- 1910
- Weight
- 690 KB
- Volume
- 29
- Category
- Article
- ISSN
- 0368-4075
No coin nor oath required. For personal study only.
β¦ Synopsis
In the k t t o r CIISU, Iiowovec, .dter about throo wwka n now standn;.d muet bo tnkon, as tho old liquor becomes grconer in colour, nhd cannot bo eccurntcb matched with liquors which hnvo only just boon spont. Tho liquors nro simply filtorcd to removo orgenic mnttor, tlio standard being plnccd in the lower trough, and tho liquor under oxsminntion in the 16 mm. trough.
Tho following serics of cornpensons by analysis shows thnt, nlthough tho mothod is not nbsolutoly accurnto, i t is quito good enough for purposes of works control. Tho annlyses wore mndo in tho usual wny by oxidising and titretion with iodino nnd thiosulphatc.
Per cent. Cr,O, dlcclly i8. Cdorimctcr. 0.503 O.fi08 0.410 0.437 0.312 0.330 0.840 0.854 0.750 0.736 0.875 0.882 0.312 0.301 0.274 0.260 . 0.302 0.294 0.249 0.233 0.196 0.187 0.252 0.237 Comparison of results obtained using two diffemnt stnndnrds. Chromic oxide. Qrnm per Utre. A . B.
π SIMILAR VOLUMES
IYtcso rcsults nro intcrcsting sinw tlicy tend to sliow tlint w r y sninll quatititics of nluminn iirc suficicnt to inhibit tlic nction of tlic sodn. Aliiminn is not often found to nny g h a t cstent in sodn, but is n frcqucnt constituent of softcncd water nnd cotton itsclf. A sccond sct of cspcrii
had rcfcrrcd t o tho prncticc of cnginccrs nnd ninnngcrs taking off tho first tnkcr of oxide purifiers,when the scCOnd tnkcr just commenced to show tlnlphurcttcd hyrlroge1i by tho lend p p c r tcst. Tlicre wns mother point to bc taken iuto nccount. Whcn the sceond lnkcr comnicncccl to show sulpliurc
COBB-SYNTHESIS OF A GLAZE, GLASS OR OTHER COMPLEX SILICATE. 709 for putting within their reach a simple method which might, at any rate. be uscd for control cxpcrimenta. JIr. J. GOLDEW Raid that Prof. Grcto had e h o m him tho rolumctric method for the estimution of phosphoric ncid rcfcrrwl to by M