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The Synthesis of 6-Formylsalicylic Acid, Esters of 6-Bromomethylsalicylic Acid, and Related Substances

✍ Scribed by Eliel, Ernest L.; Rivard, Donald E.; Burgstahler, Albert W.

Book ID
125973005
Publisher
American Chemical Society
Year
1953
Tongue
English
Weight
715 KB
Volume
18
Category
Article
ISSN
0022-3263

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## Abstract In a first step, Ξ”1‐trans‐octenoic‐3‐^14^C acid was prepared by a Grignard reaction with BaCO~3~‐^14^C and 1‐bromo‐pentane, followed by reduction of the obtained hexanoic‐1‐^14^C acid to hexanal‐1‐^14^C via the n‐hexanol‐1‐^14^C. The produced hexanal‐1‐^14^C, by condensing with malonic