The Synthesis of 5,6,7,7a,8,9,10,11-Octahydro-4H-benzo [ef]heptalene 1
β Scribed by Anderson, A. G.; Greef, Helen Frances
- Book ID
- 127094906
- Publisher
- American Chemical Society
- Year
- 1952
- Tongue
- English
- Weight
- 252 KB
- Volume
- 74
- Category
- Article
- ISSN
- 0002-7863
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The title compound, C 21 H 20 ClN 3 O 2 , was synthesized by the reaction of 4-chlorobenzaldehyde and 3-(5,5-dimethyl-3-oxocyclohex-1-enylamino)propanoic acid with malononitrile in ethylene glycol under microwave irradiation. The dihydropyridine ring has a boat conformation. The pyrimidine ring adop