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The Synthesis of 1,4-Dichlorobicyclo[2.2.1]heptane 1

✍ Scribed by Wilcox, C. F.; Zajacek, J. G.

Book ID: 126325018
Publisher: American Chemical Society
Year: 1964
Tongue: English
Weight: 394 KB
Volume: 29
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo01031a024

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Of the several methods now available for preparing derivatives of bicyclo[2.2.O]hexane, the Scherer synthesis 2,3 offers certain practical advantages. The key step in the synthetic sequence is the semi-benzilic acid ring contraction of 1,4-dichlorobicyclo[2.2.l]heptan-7one (&) with powdered sodium h