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The synthesis, characterisation and crystal structure of [Ru3(μ2-H)(CO)9(μ3-σ:σ:ν2-COPh)]

✍ Scribed by Alexander J. Blake; Paul J. Dyson; Brian F.G. Johnson; Caroline M. Martin

Publisher: Elsevier Science
Year: 1995
Tongue: English
Weight: 202 KB
Volume: 492
Category: Article
ISSN: 0022-328X
DOI: 10.1016/0022-328x(95)05442-r

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The reactions of [Pt3R~6(CO),l(p-H)3(p3-H)] (1) with PMe3 and PPh3 have produced the salts [Pt(PR3)3H]-[Pt3R~6(CO)2,(p3-H)(p-H)2]r 5a and 5d, R = Me and Ph in the yields 9% and 22%, respectively. By contrast the reaction of 1 with PPh, in the presence of Me3N0 has yielded the phosphane-substituted d