✦ LIBER ✦

The Synthesis and the Exhaustive Methylation of the cis and trans Isomers of 1,2,3,4,4a,5,6,10b-Octahydrophenanthridine and 1,2,3,4,4a,5,6,10b-Octahydrobenzo[f]quinoline 1

✍ Scribed by Masamune, Tadashi; Ohno, Masaji; Koshi, Masato; Ohuchi, Shigehiro; Iwadare, Tsukasa

Book ID: 127232396
Publisher: American Chemical Society
Year: 1964
Tongue: English
Weight: 848 KB
Volume: 29
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo01029a038

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## Abstract Die im Titel genannte Verbindung **4** ist stereoselektiv durch intramolekulare Cyclisierung des Tetrahydropyridins **3** darstellbar, das seinerseits über die Stufenfolge **5→10** aufgebaut wird. Der Aldehyd **6** ist durch Reduktion des Nitrils **5** mit Raney‐Nickel in Ameisensäure d