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The Synthesis and Structural Characterization of the New Ternary Nitrides: Ca4TiN4 and Ca5NbN5.

✍ Scribed by Janet L. Hunting; Marta M. Szymanski; Philip E. Johnson; C. Brenhin Kellar; Francis J. DiSalvo

Publisher
John Wiley and Sons
Year
2007
Weight
13 KB
Volume
38
Category
Article
ISSN
0931-7597

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Ca 4±x Ni x IrO 6 (x = 0.25, 0.5) crystallizes with trigonal (rhombohedral) symmetry in the space group R3c, Z = 6, for Ca 3.75 Ni 0.25 IrO 6 a = 9.3013(1) A Ê , c = 11.1554(1) A Ê ; for Ca 3.5 Ni 0.5 IrO 6 a = 9.2723(1) A Ê , c = 11.0825(1) A Ê . Ca 3.75 Ni 0.25 IrO 6 and Ca 3.5 Ni 0.5 IrO 6 are is