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The synthesis and ligand properties of the dihydro-bis-(1-indazolyl)borate anion

✍ Scribed by Saiyid Aftab Ahmad Zaidi; Mansoor Ahmad Neyazi

Book ID
104843875
Publisher
Springer
Year
1979
Tongue
English
Weight
245 KB
Volume
4
Category
Article
ISSN
0340-4285

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Unexpected product distributions in the synthesis of 2,6-bis-(indazolyl)pyridine and 2-(pyrazol-1-yl)-6-(indazolyl)pyridine
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a b s t r a c t Reaction of 2-bromopyridine with 2 equiv of sodium indazolide in diglyme at 140 Β°C affords 2,6-bis-(indazol-1-yl)pyridine and 2-(indazol-1-yl)-6-(indazol-2-yl)pyridine in purified yields of 24% and 68% respectively. A similar reaction, using 1 equiv of sodium indazolide at 70 Β°C, giv