The structure of β-sinensal

✍ Scribed by R.A. Flath; R.E. Lundin; R. Teranishi

• Book ID: 104250128
• Publisher: Elsevier Science
• Year: 1966
• Tongue: French
• Weight: 281 KB
• Volume: 7
• Category: Article
• ISSN: 0040-4039
• DOI: 10.1016/s0040-4039(01)99650-9

✦ Synopsis

B-Sinensal, a new oxygenated sesquiterpene, was isolated from California cold-pressed orange oil by a_ccooobination of vacu& distill&ton, silica gel chromatography, and preparative gas chromatcprephy. * The purified compound +* Is quite unstable, polymerizing rapidly at room temperature on exposure to light and air. * Carbowax 2013 on Anakrom AB, 12-ft. x l-in. column at 185O. Reference to a company or product name does 6ot finply approval or ret-ndation of the product by the U. S. Department of Agriculture to the exclusion of others that may be suitable. *+ One peak at 72 min. when analyzed on a 75-ft. x O.Ol<n. w-550 capillary columnin a Perkin-Elmer 226 gas chromatograph (programmed run).