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The structure of the methylene dibromide adduct of sporidesmin at –150°C

✍ Scribed by Fridrichsons, J. ;McL Mathieson, A.


Book ID
114519680
Publisher
International Union of Crystallography
Year
1965
Tongue
English
Weight
994 KB
Volume
18
Category
Article
ISSN
0365-110X

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The synthesis of 14C-methylene diiodide
✍ A. R. Jones 📂 Article 📅 1975 🏛 John Wiley and Sons 🌐 French ⚖ 165 KB

## Abstract Existing methods have been adapted for the small scale synthesis of the title compounds in high yield. Modification of the iodoform reaction enables 1,3‐^14^C‐acetone (I) to be converted in over 95% yield to ^14^C‐iodoform (II) which is reduced by sodium aresenite to ^14^C‐methylene dii