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The structure of a condensation product of isobutylidenecyanoacetic acid ester with cyclohexanone

โœ Scribed by Nakano, Y. ;Yatsu, M. ;Igarashi, M. ;Sato, S.

Book ID
114505031
Publisher
International Union of Crystallography
Year
1987
Tongue
English
Weight
187 KB
Volume
43
Category
Article
ISSN
0108-2701

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โœ Wayland E. Noland; Richard J. Sundberg ๐Ÿ“‚ Article ๐Ÿ“… 1962 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 277 KB

NITROMETHANE and cyclohexanone condense in refluxing solution in the presence of secondary amines to a colorless 212 product C14H20N203 (I), m.p. 270-271' (sublimes). 2,3' Secondary amines used as catalysts include piperidine4 (8-14,3 24s5 yield), piperazine (47$),5 pyrrolidine (23%),5 morpholine (2