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The Reported Adamantane Anion Radical. Its Relationship to Benzene Anion Radical

✍ Scribed by Jones, M. T.


Book ID
126445400
Publisher
American Chemical Society
Year
1966
Tongue
English
Weight
394 KB
Volume
88
Category
Article
ISSN
0002-7863

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200 mL) was acidified with 3 drops of 32% HCI and stirred for 15 min at 50Β°C (exclusion of light). After extraction with CH,CI,, the organic phase was dried (Na,SO,) and purified on silica gel (20 8). After removal of the solvent there remained 0.53 g (72%) of a crystalline product. For further puri