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The relevance of J cross-peaks in two-dimensional NOE experiments of macromolecules

✍ Scribed by S Macura; K Wüthrich; R.R Ernst

Publisher
Elsevier Science
Year
1982
Weight
470 KB
Volume
47
Category
Article
ISSN
0022-2364

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Suppression of direct peaks in two-dimen
Suppression of direct peaks in two-dimensional heteronuclear NOE spectra. Sensitivity-enhanced detection of weak indirect and relay peaks
✍ Katalin E. Kövér; Gy. Batta 📂 Article 📅 1988 🏛 John Wiley and Sons 🌐 English ⚖ 319 KB

A spin-echo sequence is proposed for the suppression of the generally unnecessary strong direct cross-peaks in two-dimensional heteronuclear NOE and relayed incoherent transfer spectroscopy. The procedure also increases the intensity of 'remote peaks,' thereby enhancing the sensitivity of these tech