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The relative and absolute configurations of stereocenters in caryophyllose

✍ Scribed by Matteo Adinolfi; Maria M. Corsaro; Cristina De Castro; Antonio Evidente; Rosa Lanzetta; Lorenzo Mangoni; Michelangelo Parrilli

Publisher
Elsevier Science
Year
1995
Tongue
English
Weight
508 KB
Volume
274
Category
Article
ISSN
0008-6215

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✦ Synopsis

The complete stereochemistry of the monosacccharide 3,6,10-trideoxy-4-C-[(R)-l-hydroxyethyl]-D-erythro-D-gulo-decose, named caryophyllose, obtained from the lipopolysaccharide fraction of Pseudomonas caryophylli is reported. The relative stereochemistry was inferred by 1H NMR analysis and the absolute configuration was independently elucidated by Mosher's and Exciton Chiral Coupling methods.

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