The title compound, C 21 H 19 N 5 , has been synthesized and characterized by single-crystal X-ray diffraction. The dihedral angle between the benzene and triazole rings is 123.0 (5) . The triazole ring forms dihedral angles of 36.5 (5) and 50.1 (5) with the two pyridyl rings.
The reduction products of 2-phenyl-1,3-di(4-pyridyl)-2-propanol
✍ Scribed by M. E. Derieg; B. Brust; R. Ian Fryer
- Book ID
- 112121433
- Publisher
- Journal of Heterocyclic Chemistry
- Year
- 1966
- Tongue
- English
- Weight
- 506 KB
- Volume
- 3
- Category
- Article
- ISSN
- 0022-152X
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê Disorder in main residue R factor = 0.064 wR factor = 0.136 Data-to-parameter ratio = 12.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
In the title compound, C 21 H 19 N 5 , the pyridyl groups and the benzene ring lie in a propeller arrangement around the central 1,2,4-triazole ring, minimizing the steric effects among these rings. ## Experimental Compound (I) was synthesized by the reaction of equivalent amounts of p-isopropylp