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The reaction of singlet oxygen with 2-phenylcycloalkenes possessing small and common rings

✍ Scribed by Charles W. Jefford; Christian G. Rimbault

Publisher
Elsevier Science
Year
1976
Tongue
French
Weight
135 KB
Volume
17
Category
Article
ISSN
0040-4039

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The Reaction of Singlet and Triplet Oxyg
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## Abstract The reaction of singlet oxygen with 2‐phenylnorbornene (**1**) in aprotic solvents gives 3‐formylcyclopentyl phenyl ketone (**2**) (10%) and uncharacterized polymer (90%). When methanol is used as solvent, __endo__‐2‐phenyl‐__exo__‐2‐methoxy‐__exo__‐3‐hydroperoxynorbornane (**4**) and _

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✍ Charles W. Jefford; André F. Boschung; Robert M. Moriarty; Christian G. Rimbault 📂 Article 📅 1973 🏛 John Wiley and Sons 🌐 German ⚖ 642 KB

## Abstract The reaction of photogenerated singlet oxygen with α‐ and β‐pinenes has been carefully re‐examined. α‐Pinene almost exclusively (99.3% yield) furnishes __trans__‐3‐hydroperoxy‐pin2(10)‐ene. However, detectable amounts of the three other possible products are also found, viz., __cis__‐3‐