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The Reaction of Carboxylic Acid Esters with RfMgBr: A Convenient Synthesis of Perfluoroalkyl Ketones

✍ Scribed by Can Xue; Guangke He; Chunling Fu; Liqin Xue; Zhenyang Lin; Shengming Ma

Publisher: John Wiley and Sons
Year: 2010
Tongue: English
Weight: 233 KB
Volume: 2010
Category: Article
ISSN: 1434-193X
DOI: 10.1002/ejoc.201000887

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## Abstract Polycyclic ‘cage’ ketones, such as pentacyclo[5.4.0.0^2,6^.0^3,10^.0^5,9^]undecan‐8‐one (**10**), pentacyclo[5.4.0.0^2,6^.0^3,10^.0^5,9^]undecane‐8,11‐dione (**11**), and adamantan‐2‐one (**16**) were treated with the nucleophilic dimethoxycarbene (DMC; **1**), which was generated therm