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The reaction of carbonyl cyanide phenylhydrazones with thiols

✍ Scribed by Drobnica, LÌ.; Å turdÃk, E.

Book ID: 120571316
Publisher: Elsevier Science
Year: 1979
Tongue: English
Weight: 850 KB
Volume: 585
Category: Article
ISSN: 0304-4165
DOI: 10.1016/0304-4165(79)90091-6

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residue remaining on evaporation was chromatographed on 850 g of silica gel (column 4x90 cm) with hexane/acetone (100: 3). The first 300 ml of eluate contained 10.9 g of crude product (30). This was taken up in ether, and washed with 1 % hydrochloric acid and 1 % sodium hydrogen carbonate solution;