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The reaction of carbon disulfide with α-diazo ketones. The structure and stereochemistry of the racemic product from 2-(p-bromophenyl)-2-diazoacetophenone

✍ Scribed by K. Dichmann; D. Bichan; S.C. Nvburg; Peter Yates

Publisher: Elsevier Science
Year: 1971
Tongue: French
Weight: 162 KB
Volume: 12
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(01)97253-3

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✦ Synopsis

The product formed from 2-diazo-2-phenylacetophenone (I) and carbon disul-

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## Carbon disulphide inserts into the Pt-H bond oj trans-{PtH,[P(C~,1)3]2} to give trans-{PtH(S,CH) [P(CJ113J2}. The X-ray structure shows that the -S2CH group is bonded to the metal through a sulfur atom as a monodentate thioformate anion. The kinetics of the carbon disulfide insertion have been in