𝔖 Bobbio Scriptorium
✦   LIBER   ✦

The properties of thiobenzyl esters of the P(III) acids. Part I. The study of the reaction mechanism of 2-benzylthio-4,5-benzo-1,3,2-dioxaphospholane with ketones and oxygen by CIDNP 31P

✍ Scribed by Yana A. Drozdova; Alexander R. Burilov; Michael A. Pudovik; Rafinad M. Gainullin; Akhat V. Il'Yasov


Publisher
John Wiley and Sons
Year
1992
Tongue
English
Weight
374 KB
Volume
3
Category
Article
ISSN
1042-7163

No coin nor oath required. For personal study only.

✦ Synopsis


R 2 PC1 2-Benzylthio -4,5 -benzo-1,3,2-dioxaphospholane reacts with oxygen to form the corresponding thiophosphonate, dithiophosphate and pyrophosphite. The reaction was found to be of a radical nature. The mechanism is suggested to i n m l w an initial electron transfer with suitable subsequent transformations. The interaction of the title compound with mrious ketones in a pure oxygen atmosphere was studied by the CIDNP method.