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The preparation of mixed benzyl pyridine isomers on a pilot plant scale

✍ Scribed by Hands, C. H. G. ;Whitt, F. R.

Publisher
Wiley (John Wiley & Sons)
Year
1947
Weight
331 KB
Volume
66
Category
Article
ISSN
0368-4075

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✦ Synopsis

Abstract

A semi‐technical method of preparing a mixture of 2 and 4‐benzyl pyridines at the rate of several cwt. per week utilizing the reaction between benzyl chloride and pyridine is described Satisfactory control of the reaction on the 1 cwt. batch size was obtained by the use of circulating hot oil as the reaction vessel heating medium.

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✍ Hands, C. H. G. ;Whitt, F. R. 📂 Article 📅 1948 🏛 Wiley (John Wiley & Sons) ⚖ 459 KB 👁 1 views

Above 38o0-42oo, the reaction, also leads to elementary carbon formation. Schmidt,8 however, in an X-ray examination, failed to find any evidence for the existence of the higher carbide Ni,C,. In considering whether Bahr and Bahr's mechanism can be applied to interpret the results obtained with th