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The Preparation of Geminally Substituted 4-Bromobutylamines. I. 4-Bromobutylamine and 4-Bromo-1,1-dimethylbutylamine 1

✍ Scribed by Brown, Ronald F.; von Gulick, Norman M.


Book ID
127057695
Publisher
American Chemical Society
Year
1955
Tongue
English
Weight
727 KB
Volume
77
Category
Article
ISSN
0002-7863

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## Abstract The reaction of benzoyl isothiocyanates and methoxycarbonyl isothiocyanate with 4‐amino‐4,5‐dihydro‐3‐(methylthio)‐1,2,4‐triazin‐5‐ones in acetonitrile gave several substituted 4__H__‐1,3,4‐thiadiazolo[2,3‐__c__]‐1,2,4‐triazin‐4‐ones VIa‐h instead of the expected thioureas. In addition,