✦ LIBER ✦

The Preparation of Certain Substituted Alkenols and Their Chloro Analogs

✍ Scribed by Semeniuk, Fred ;Jenkins, Glenn L.

Publisher: Elsevier
Year: 1948
Weight: 378 KB
Volume: 37
Category: Article
ISSN: 0095-9553
DOI: 10.1002/jps.3030370309

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✦ Synopsis

ERTAIN olefinic halogenated compounds are of significance from the standpoint of preparative methods proposed for them and of their possible utility as intermediates in the synthesis of new types of physiologically active compounds. These halogenated compounds are the 4-substituted-l-halo-2butenes, which are satisfied by the general formula:

Q-CH~-CH=CH-CH2-Xl where Qis any substituent not necessarily hydrocarbonaceous. Those selected for preliminary study constitute a fairly uniform series of five in which the various values of Qare methyl-, cyclohexyl-, phenyl-, anaphthyl-and o-ethoxyphenyl-, and in which the halo-substituent is chloro-.

3,4-Epoxy-l-butene (Butadiene mon-*

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