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The Preparation of 1-C 14 -Labeled Glucose, Mannose and Fructose 1

✍ Scribed by Hers, H. G.; Edelman, J.; Ginsburg, V.

Book ID
120347091
Publisher
American Chemical Society
Year
1954
Tongue
English
Weight
276 KB
Volume
76
Category
Article
ISSN
0002-7863

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## Abstract The preparation of ^14^C‐labelled dimethylsilane‐1, 1‐diol in two steps from ^14^C‐labelled diphenyldimethylsilane is described. Aluminum chloride catalyzed protodesilylation of diphenyldimethylsilane with HCl in dichloromethane or dimethyldichlorosilane at 0–5Β°C affords labelled dimeth