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The polycondensation of bis-(β-hydroxyethoxymethyl) tetramethyl disiloxane with dicarboxylic acids

✍ Scribed by K.A. Andrianov; L.I. Makarova; N.M. Zharkova


Book ID
118355331
Publisher
Elsevier Science
Year
1962
Weight
329 KB
Volume
3
Category
Article
ISSN
0032-3950

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When O,OЈ-Bistrimethylsilyl catechol (BTSC) was polycondensed with adipoyl chloride in o-dichlorobenzene the 10-membered cyclic monomer was the main reaction product regardless of the concentration. Even the polycondensation in bulk yielded the macrocyclic monomer as the main product. Polycondensati