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The photochemical 1,3-cycloaddition of carbonyl compounds with oxiranes: a competitive cleavage of carboncarbon and carbonoxygen bonds in ethyl 2-methyl-3-phenylglycidate

✍ Scribed by J. Kagan; J.T. Przybytek; B.E. Firth; S.P. Singh

Publisher: Elsevier Science
Year: 1972
Tongue: French
Weight: 203 KB
Volume: 13
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(01)85188-1

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✦ Synopsis

reoeived in UX for publication 13 IVovambsr 1972) When a benzene solution of either cis &-c) or trans 2-methyl-3-phenylglycidate 2-g) was irradiated in benzene under N 2 at 254 nm for 48 hrs., about 20% conversion to a complex mixture was observed. Silica gel chromatography afforded only one crystalline product m.p. 103-104: (for example, 30 mg from

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