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The Occurrence of Metastable Tetragonal Zirconia as a Crystallite Size Effect

✍ Scribed by Garvie, Ronald C.

Book ID
115480972
Publisher
American Chemical Society
Year
1965
Tongue
English
Weight
594 KB
Volume
69
Category
Article
ISSN
0022-3654

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Crystallite Size Effect on the Tetragona
Crystallite Size Effect on the Tetragonal-Monoclinic Transition of Undoped Nanocrystalline Zirconia Studied by XRD and Raman Spectrometry
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Two powdered batches of undoped zirconia, prepared by spray pyrolysis and characterized by 6.9 and 13.2 nm average crystallite size were annealed for di4erent temperatures and for di4erent times. The tetragonal+monoclinic phase transformation was monitored by Raman spectroscopy and X-ray di4raction.