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The Nitration of Toluene with Alkyl Nitrates and Polyphosphoric Acid 1

✍ Scribed by Tsang, S. M.; Paul, A. P.; DiGiaimo, M. P.


Book ID
127200622
Publisher
American Chemical Society
Year
1964
Tongue
English
Weight
528 KB
Volume
29
Category
Article
ISSN
0022-3263

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Nitration of Alkyl Benzoates with Mixed
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## Abstract The nitration of (substituted) benzoic acid esters is usually performed in fed‐batch operation. The ester is solved in sulfuric acid charged first. The nitric acid dosed keeps the reaction temperature under control. The safety regarding uncontrolled reaction conditions was investigated