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The Newman−Kwart Rearrangement: A Microwave Kinetic Study

✍ Scribed by Gilday, John P.; Lenden, Philip; Moseley, Jonathan D.; Cox, Brian G.

Book ID: 115451968
Publisher: American Chemical Society
Year: 2008
Tongue: English
Weight: 154 KB
Volume: 73
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo702633g

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## Abstract The 2‐alkyl‐ and 2,6‐dialkylbenzenesulfonyl chlorides 5a‐f were obtained in high yield by chlorination of the correspondingly substituted S‐aryl N,N‐dialkylthiocarbamates 4a‐g. These precursors have been synthesized via the Newman‐Kwart rearrangement of the corresponding O‐aryl N,N‐dial